九州大学 · 工学
Kawahara教授の研究室では、高張力性ステンレス鋼の微視的メカニズムに着目し、窒素添加が微細組織と力学的特性に与える影響を、電子顕微鏡法と原子プローブトモグラフィーを用いて原子スケールで解明しています。特に、積層欠険エネルギー(SFE)の変化が塑性変形メカニズムや高温強度に与える影響を重点的に研究しており、窒素とクロムの短距離秩序や不純物原子と不純物欠陊の相互作用の解明を目指しています。
Figures are computed from collected data and may differ slightly.
Austenitic stainless steels have superior room temperature and high temperature strengths, strongly influenced by stacking-faults in the steel microstructure. Nitrogen addition makes substantial contribution to room temperature and high temperature strengths, so it is essential to consider the effect of nitrogen on the stacking-fault energies (SFE) to understand strength mechanism of the steel and to enhance the strength. In this study, SFE were measured by weak-beam TEM method, and deformation
Combined addition of interstitial-substitutional elements has been acknowledged to contribute to the increase in the strengths of steels. For further improvements in mechanical properties, their atomic-scale interaction mechanisms with dislocations are required to be examined. In this study, both high-resolution transmission electron microscopy and atom-probe tomography were used to correlate interstitial-substitutional elements with dislocation characteristics in austenitic stainless steels. Th
The structures of carbon clusters and carbides in a low-carbon ferritic steel were investigated at atomic-scale by annular dark-field scanning transmission electron microscopy. In the low-carbon ferritic steel aged at 473 K for 1 h, some homogeneously dispersed ε-carbides were formed within the matrix as closely spaced granules aligned to <001> of the ferrite matrix, and others were heterogeneously formed on AlN precipitates. The ε-carbides formed on AlN precipitates were coexisted with carbon c
The stacking-fault energies (SFE) were measured by weak-beam TEM method, and deformation mechanisms in room and high temperature were characterized in terms of the effect of nitrogen addition on SFE in Si-added austenitic stainless steel (Fe-19%Cr-13%Ni-0.05%C-3%Si-x%N). Nitrogen addition resulted in decrease of SFE and changing the dislocation configuration from tangled to planar in room temperature. In high temperature, nitrogen addition resulted in the increase of dislocation density in the s
Abstract Interstitial-substitutional pairs have been acknowledged to contribute to the increase in the strengths of steels. For further improvements in mechanical properties, their atomic-scale structures and interaction mechanisms with defects are required to be examined. In this study, both high-resolution transmission electron microscopy and atom-probe tomography were used to correlate interstitial-substitutional pairs with defect characteristics in austenitic stainless steels. Three types of
Planar slips have been frequently recognized in nitrogen-added austenitic stainless steels, and often discussed in terms of stacking-fault energy (SFE). On the other hand, nitrogen addition promotes the formation of N-Cr short-range order (SRO), which has been proposed to cause the planar slips. In this study, a chromium-free Fe-N binary austenite with 2.4 mass% of fully solid-solutioned N was fabricated to simplify the relationship among deformation structures, SFE and N-Cr SRO. The Fe-N alloy
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